4.1 Inorganic chemistry of group 1 and 2

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    Describe and explain the trend in ionisation energy down Group 2.

    The ionisation energies of group 2 elements decreases down the group. This is because - The atomic radius is larger as there is +1 quantum shell each time - Therefore increased shielding to the outer electron - These factors outweigh the increase in proton number

    Describe and explain the trend in reactivity down group 2 elements.

    General increase in reactivity - Due to differences in metallic radii - Sum of first and second ionisation energies decreases

    Give the general equation for the reactions of Mg, Ca, Sr and Ba (represented by M) with oxygen. Include state symbols.

    2M(s) + O2(g) ——> 2MO(g)

    What would you observe when group 2 metals react with oxygen in the presence of a Bunsen flame?

    - extremely bright flame - formation of a white solid powder

    Why do group 2 metals appear dull?

    They react slowly with oxygen without the presence of a flame to form a dull oxide layer, preventing further reaction.

    Why is barium often stored in oil?

    To prevent reaction with oxygen or water vapour in the air.

    Give the general equation for the reaction of group 2 metals with chlorine when heated. Include state symbols.

    M(s) + Cl2(g) ——> MgCl2(s)

    Give the general equation for the reaction of group 2 metals with water.

    M(s) + 2H2O(l) ——> M(OH)2(aq) + H2(g)

    What group 2 metals forms a solid metal hydroxide when reacted with water?

    Calcium hydroxide (sparingly soluble in water) therefore the vessel will go cloudy.

    What would you observe when group 2 metals react with water?

    Effervescence

    Why are group 2 oxides known as basic oxides?

    They react with water to form alkalis

    What is the general equation and ionic equation for the reaction of group 2 oxide with water.

    MO(s) + H2O(l) ——> M(OH)2(aq/s) O2- + H2O —> 2OH-

    Describe and explain the trend in solubility of group 2 hydroxides.

    Increases down the group

    How do you test for carbon dioxide? Give the equation with state symbols.

    Bubble gas through limewater (hydrated calcium hydroxide). Limewater will go cloudy if CO2 present. CO2(g) + Ca(OH)2(aq) ——> CaCO3(s) + H2O(l)

    Give a general equation for the reaction of group 2 oxides with acids.

    MO + acid ——> metal salt + water

    Give the general equation for the reaction of group 2 hydroxides with water.

    M(OH)2 + acid ——> metal salt + water

    Give the trend in then solubility of group 2 sulfates.

    Soluble: Magnesium sulfate Sparingly soluble: Calcium sulfate Insoluble: Strontiium and barium sulfate.

    Describe the test for sulfate ions. Give the ionic equation including state symbols.

    - add acidified barium chloride / nitrate solution, white barium sulfate ppt will form Ba 2+ (aq) + SO4 2- (aq) ——> BaSO4(s)

    Why must the barium chloride/nitrate solution be acidified?

    To prevent the formation of barium carbonate and forming a false positive white ppt.

    What is thermal stability?

    Indication of how stable a compound is when it is heated. Something which does not undergo thermal decomposition would be classed as thermally stable.

    Why do group 2 metal carbonates/nitrates decompose and NOT melt?

    Complex carbonate /nitrate ions decompose into more stable compounds, rather than being free ions in the molten phase.

    Describe and explain the trend in thermal stability of group 2 carbonates / nitrates.

    As you go down group 2, thermal stability increases. This is because: - The metal cations become less charge dense as their ionic radii increase - Therefore the polarising power of the cation decreases - Therefore the N-O bonds / C-O bonds are weakened/polarised/distorted less.

    Give the general equation for the thermal decomposition of group 2 nitrates.

    Metal nitrate ——> metal oxide + NO2 + O2

    What observation is made upon thermal decomposition of group 2 nitrates?

    Brown fumes (nitrogen dioxide)

    Give the general equation for the thermal decomposition of group 1 nitrates.

    Metal nitrate ——> metal nitrite + O2

    What is the exception for thermal decomposition of group 1 nitrates and carbonates?

    Lithium nitrate will decompose the same way as group 2 nitrates as Li+ is an incredibly charge dense ion therefore reacts similarly to charge dense 2+ group 2 ions.

    What is the general equation for the thermal decomposition of group 2 carbonates?

    metal carbonate ——> metal oxide + CO2

    What is the observation of thermal decomposition of group 2 carbonates?

    There is no visible change as CO2 is colourless and both the carbonates and oxides are white solids.

    Do group 1 carbonates thermally decompose?

    Yes - but at VERY high temperatures.

    What is a flame test used for?

    To distinguish metal ions in compounds.

    How do you carry out a flame test?

    - wear safety goggles - add a few drops of conc. HCl to the metal sample so some dissolves, allowing the formation of metal chlorides. - Dip a clean nichrome wire loop into concentrated HCl, then into the sample - Place the wire INTO a roaring (blue) Bunsen flame and observe the colour.

    Why is the formation of metal chlorides essential in a flame test?

    Chlorides are the most volatile salts therefore produce the best results.

    What are the problems associated with flame tests?

    - many compounds contain sodium impurities, so sodium colours often mask other colours. - colour observation is subjective

    What is the flame test colour of a lithium ion?

    Red

    What is the flame test colour of a sodium ion?

    Yellow-orange

    What is the flame test colour of a potassium ion?

    Lilac

    What is the flame test colour of a rubidium ion?

    Red-purple

    What is the flame test colour of a caesium ion?

    Blue - violet

    What is the flame test colour of a beryllium ion?

    No colour

    What is the flame test colour of a magnesium ion?

    No colour

    What is the flame test colour of a calcium ion?

    Brick red

    What is the flame test colour of a strontium ion?

    Crimson red

    What is the flame test colour of a barium ion?

    Apple green

    Why do flame tests produce colour?

    - electrons absorb heat energy and are 'excited' to a higher energy level - electrons return to ground state releasing energy which corresponds to a specific wavelength(s) of light. - if the wavelength of light is within the visible spectrum, a colour will be observed.

    How do you test for an ammonium ion? (2 ways).

    - Add warm NaOH releasing ammonia gas: NH4+ + OH- —-> NH3(g) + H2O Either: - hold damp litmus paper above, turns litmus paper red to blue as it is alkali OR - HCl gas reacts with ammonia gas to form white, misty NH4Cl fumes: NH3(g) + HCl(g) —-> NH4Cl